Synthesis and Characterization of TiO2 /Fe3O4 Composites Using Sonication Method

Elsa Avrilia Putriani; Noor Hindryawati; Hajar Anuar

doi:10.55927/ijis.v5i1.807

Authors

Elsa Avrilia Putriani Universitas Mulawarman
Noor Hindryawati Mulawarman University
Hajar Anuar Mulawarman University

DOI:

https://doi.org/10.55927/ijis.v5i1.807

Keywords:

Composite, TiO2 , Fe3O4, Sonication

Abstract

TiO₂/Fe₃O₄composite was synthesized by sonication method using mass ratio of 10:1 then calcined at 400ºC for 2 hours. Characterization of TiO₂/Fe₃O₄composite was carried out using X-Ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR) and Scanning Electron Microscope (SEM) instruments. The results of characterization of TiO₂/Fe₃O₄composite using XRD showed diffractogram results with a collection of Fe₃O₄ phases and TiO₂ phases with a crystallinity value of 64.7%. FTIR analysis showed Ti-O-Ti vibrations appeared in the range of 700-900 cm-1 and absorption bands from Fe-O vibrations appeared at a peak around 600 cm-1. SEM analysis showed the morphology of TiO₂/Fe₃O₄composite with Fe₃O₄particles attached to the surface of TiO₂particles and forming a rough surface.

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